Dental care liquids with small and dispersed particles
Products/Oral Care
Dental care liquid system

NatFibra OL

Oral care with NatFibra® fiber suspension stabilizer

To improve the distribution of insoluble powders, fragrance microdrops and other dispersive components in continuous aqueous case.

INCI
CELLULOSE
microfibrils diameter
About 20-40 nm
Fibre length
More than μm
Main uses
Suspended dental care liquid
01 / Product Overview
Microfibrils suspended structure

A continuous microfibril network for liquid oral-care systems

NatFibra® OL is based on NatFibra® fiber from fermentation sources. Fibres are dispersed and interwoven in the liquid phase, providing structural support for particles and droplets.

System viscosity, mobility and oral use are affected by the complete formulation and should be determined in combination with product additions, particle characteristics and processing conditions.

Type of product
Oral care with NatFibra® fiber suspension stabilizer
Sources of material
Bio-cellulose
Structural characteristics
A continuous network of three-dimensional microfibrils in a liquid phase
Apply Object
Insoluble powders, fragrance microdrops and other dispersed components
02 / Material Structure NatFibra® fiber

20-40 nm microfibrils form a continuous network in the liquid phase

NatFibra® fiber is fermented from sugar sources and cellulose molecular chains are connected by glucose units via β-1,4 glycosidic bond and further assembled as nanofibrils. Higher spect rateo allows material to form more contact points in aqueous case.

Visual representation of the NatFibra® fiber network and dispersed particles
01

Particle support

Limit the transport of insoluble powder and decorative particles in static conditions.

02

Droplet distribution

Improve the spatial distribution of fragrance microdrops or other dispersed droplets in successive aqueous cases.

03

Low shear structure

Establish internal structures and retain the flow status required for liquid systems.

NatFibra® Fiber and cellulose chain structure
Left: NatFibra® fiber micrograph; right: cellulose chain and nanofibre structure.
NatFibra® fiber 3D network
high-aspect-ratio microfibrils are interwoven into a network, with dispersed clusters located between network holes.
03 / Preparation process Fermentation and Purification

Fermentation, purification and application formulation

Fragmentation, effective solid content and final product composition are based on current product specifications.

  1. 01

    Fermentation

    Sugar sources and germs enter the fermentation stage, forming the bio-cellulose.

  2. 02

    Purification

    Elimination of cultures and fermentation residues and acquisition of pure cellulose material.

  3. 03

    Application formulation

    Material formation based on the use requirements of the dental care liquid system.

  4. 04

    Quality control

    Complete formulation, quality indicator recognition and packaging.

Comparison of samples of particulate liquid systems for oral care
04 / Sample observation Particle Distribution

The distribution of particles depends on the network structure and the condition of the formation

The particles in the left sample are concentrated mainly at the bottom of the container; the particles in the right sample are distributed in the liquid phase. The group did not include basic additions, particle properties, storage temperature and observation time.

The official certification shall be based on the stability of the particle density, particle size, shape and addition, and shall not directly consider the state in the photograph as the result of the shelf period.

Scope of evaluationParticle distribution, sedimentation at the bottom, gathering, dispersing.
05 / adaptation Mobility and compatibility

Evaluate flow behavior and formulation compatibility together

The structural effects of the material are not the only mechanism based on the traditional high viscosity, but do not mean that the viscosity of all of it remains unchanged. The practical application window is confirmed by a gradient test.

01

pH

Recognition of appearance, particle distribution, viscosity, yield condition and storage stability.

02

electrolyte

Comparison of network structures, particle deposition and liquid droplets before and after salt addition.

03

Temperature

Observe the appearance and current state of the heat, high temperatures, low temperatures and high cryogenic cycles.

04

Shear

Validation of the impact of decentralized speed and time on network recovery and the homogeneity of finished products.

05

Formulation components

Assess the compatibility of perfumes, surfactants, preservatives, sweets and functional components.

It is recommended to record the flows and continuity of Brookefield viscosity, yield condition, touch recovery, flow curves, and during dumping, pumping or ejection.

06 / Water Holding Structure Water combined with free water

Hydroxyl groups, pores and the continuous network influence water distribution

Hydroxyl radicals on cellulose chains form hydrogen keys with water molecules. The pore and continuous network between microfibrils together influence the distribution of water in materials in combination with free water.

98%bio-cellulose materials with maximum water retention
>100 ×Material holding data in the cited study

The above values correspond to the bio-cellulose material and the corresponding research conditions and are not equivalent to the conclusion of oral wetting or efficacy of the finished NatFibra® OL product.

bio-cellulose combines water with free water structures
Hydrogen keys between cellulose chains and microfibrils network influence the distribution of water in combination with free water.
microbial cellulose Water Research Documentation
Documentary information on the microbial cellulose Water Capacity Study.
07 / Dispersion Model Pickering Dairy Model

Microfibrils contribute to the oil-water interface and continuous aqueous structure

The NatFibra® fiber of high-aspect-ratio can be distributed over the oil-water area and, together with a continuous three-dimensional network of aqueous phasies, restrict the movement of oil droplets. This structure can be used for decentralized system studies with perfume oil or other oil case components.

NatFibra 5% Soya oil model sample
5%Soya oil model sample
NatFibra 10% Soya oil model sample
10%Soya oil model sample
NatFibra 15% Soya oil model sample
15%Soya oil model sample
NatFibra 20% Soya oil model sample
20%Soya oil model sample

In this model, samples that add more than 10% to NatFibra are marked as stable emulsion. The samples did not show the oil water ratio, average process, storage temperature, observation time and evaluation method, and the graphical concentration did not represent the recommended additions to NatFibra® OL oral care.

Laboratory application for dental care liquid system
08 / Scope of application Dental care liquids

For dental care liquids containing particles or droplets

Specific product patterns and permitted raw materials should conform to the oral care regulations and product safety requirements of the target market.

01

Insoluble powder

For dental care liquids that require control of powder deposition and bottom concentrations.

02

Decorative particles

Liquid systems that require the maintenance of a spatial distribution and appearance of particles.

03

Contains fragrance droplets

Water-based dispersion systems for aromatic microdrops or a small amount of oil case.

04

Low-viscosity liquid systems

Formulation for both particle distribution and dumping, pumping or ejection.

09 / Technical information Parameters and Authentication

Additions and processes are determined according to the target system

The available product information does not give a uniform recommended addition applicable to the entire oral care system. It is proposed to set an addition gradient based on the requirement of a solid content, particle load, droplet ratio, target flow status and stability.

Product specifications

Product name
NatFibra® OL
INCI
CELLULOSE
Material type
fermentation source NatFibra® fiber
Fibre diameter
About 20-40 nm
Fibre length
More than μm
Network structure
A continuous network of three-dimensional microfibrils in a liquid phase
Main functions
Support particles and fluid droplets to improve the static status of dispersed components
Main applications
Dental care liquid dispersion system

Formulation-development checklist

  1. 01

    Predispersion, order of additions, cut speed and cut time

  2. 02

    Particle density, particle size, shape and addition

  3. 03

    Consistency of perfume, surfactants, electrolytes and preservative systems

  4. 04

    Force pH, ion strength and processing temperature

  5. 05

    Low shear viscosity, yield style, touch recovery and flow curve

  6. 06

    Centrifugal, high-temperature, low-temperature, frozen and high-temperature cycle stability

  7. 07

    The inner wall of the bag is attached, bottom sedimentation, redispersion and filling.

  8. 08

    Microbiological control, preservation challenges and oral exposure safety assessment

Product appearance, effective solid content, finished product pH, microbiological indicators, shelf life, recommended additions and standard additives are based on the latest product specifications and technical documents.